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I. SUGAR AND SUGAR BY-PRODUCTS |
||
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A. Raw Sugar |
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|
1.Moisture |
Vacuum Oven Drying (PNS 1097:1993) |
400.00 |
2.Polarization |
Wet Lead (PNS 1097:1993) |
400.00 |
3.Ash |
Sulfated (ICUMSA 1/3/4/7/8-11) |
400.00 |
4.Grain Size |
% through 28 Mesh Tyler Sieve (NYSTL method)/PNS 1097:1993 |
400.00 |
5.Color |
Modified method 4 (PNS 1097:1993) |
|
5.1 Affined |
|
400.00 |
5.2. Whole Raw |
|
400.00 |
6.Sucrose |
Walker's Inversion |
650.00 |
7.Reducing Sugar |
Lane & Eynon/Constant Volume (ICUMSA GS1/3/7-3) |
600.00 |
8.Dextran |
a) Robert's Method - AOAC |
1,000.00 |
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b) Modified Alcohol Haze (ICUMSA GS1-15) |
750.00 |
9.pH |
Potentiometric (ICUMSA GS1/2/3/4/7/8-23 |
400.00 |
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B. Refined Sugar |
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1. Moisture |
Oven Drying (ICUMSA GS2/1/3-15) |
400.00 |
2. Polarization |
Non-lead (OCHPSI) |
400.00 |
3. Sucrose |
Walker's Inversion (PNS 1098:1993) |
650.00 |
4. Ash |
Conductimetric (ICUMSA GS2/3-17) |
400.00 |
5. Color |
PNS 1098:1993 |
400.00 |
6. Reducing Sugar |
Lane & Eynon (PNS 1098:1993)/ICUMSA GS2/3-5 |
600.00 |
7. Floc Test |
ICUMSA 79/PNS 1098:1993 |
400.00 |
8. Sulfur Dioxide |
Rosaniline colorimetric (ICUMSA GS2/1/7-33) |
750.00 |
9. Iron |
Colorimetric (ICUMSA GS 2/3/7/8-31) |
750.00 |
10. Microorganism |
Pour plate (PNS 1098:1993) |
1,400.00 |
11. Contaminants |
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|
11.1. Lead |
a) AAS (ICUMSA GS 2/3-23) |
1,800.00 |
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b) Colorimetric (ICUMSA 2/1/3-27) |
1,500.00 |
11.2. Arsenic |
a) AAS (ICUMSA GS 2/3-23) |
1,800.00 |
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b) Colorimetric (ICUMSA 2/3-25) |
1,100.00 |
12. Copper |
a) AAS |
1,800.00 |
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b) Colorimetric (ICUMSA 2/3-29) |
1,000.00 |
13. Grist Size |
MA/CV (ICUMSA GS2-37) |
400.00 |
14. Quarterly ammonium Compound
(QAC) |
Coca Cola/Bulletin#32 Nutritive Sweetener Test Methodologies, SW-L-025 |
1,700.00 |
15. Sediment |
Membrane Filtration (PNS 1098:1993) |
600.00 |
16. Residue on ignition |
U.S. Pharmacopoeia |
400.00 |
17. Chlorides |
U.S. Pharmacopoeia/Turbidity Test |
400.00 |
18. Sulfates |
U.S. Pharmacopoeia/Turbidity Test |
400.00 |
19. Calcium |
U.S. Pharmacopoeia/Turbidity Test |
400.00 |
20. Barium |
British Pharmacopoeia/Opalescence Test |
400.00 |
21. Dextrin |
British Pharmacopoeia/Color Test |
400.00 |
22. Acidity & Alkalinity |
British Pharmacopoeia/Color Test |
400.00 |
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C. Pre-mixes/Dry mixes/ Concentrates |
|
. |
1. Sucrose, glucose, fructose |
HPIC (standard calibration) CarboPac PA1, ECD-PAD1 |
975.00 |
| . | . |
. |
D. Molasses | . |
. |
1. Brix |
Hydrometer |
400.00 |
2. Pol |
Dry Lead |
400.00 |
3. Sucrose |
Walker's Inversion |
650.00 |
4. Reducing Sugar |
Lane & Eynon Constant Volume (ICUMSA GS4/3-3) |
600.00 |
5. Total Solids |
Oven drying on sand |
700.00 |
6. Ash |
Sulfated (ICUMSA GS 3/4/7/8-11 |
400.00 |
7. Specific Gravity |
Hydrometer/pycnometer |
400.00 |
8. Refractive Index |
Refractometer |
400.00 |
9. Unfermentable Reducing Sugar |
Titrimetric/OMCC revised |
900.00 |
10. Suspended Solids |
Oven drying/OMCC revised |
400.00 |
11. pH |
Potentiometric |
400.00 |
| . | . |
. |
E. Muscovado | . | . |
1. Brix |
Hydrometer |
400.00 |
2. Pol |
Dry Lead |
400.00 |
3. Sucrose |
Walker's Inversion/OMCC |
650.00 |
4. Reducing Sugar |
Lane & Eynon Constant Volume |
600.00 |
5. Total Solids |
Oven drying on sand/OMCC |
700.00 |
| . | . | . |
II. AGRO-INDUSTRIAL PRODUCTS | ||
A. Feeds and Fertilizer | . |
. |
1. Nitrogen |
Kjeldahl Digestion: AOAC 15th ED. 988.05 |
500.00 |
2. Phosphorus |
UV-Vis Spectrophotometric:AOAC 15th ed. 965.17 |
400.00 |
3. Inorganic Material (Potassium) |
FES: 15th ed. 956.01 |
1,250.00 |
4. Calcium |
AAS: AOAC 15th ed. 975.03 |
1,000.00 |
5. Magnesium |
AAS: AOAC 15th ed. 975.03 |
1,000.00 |
6. Organic Matter |
Walkley-Black 1 |
350.00 |
7. Moisture |
Oven-Drying:AOAC 15th ed. 930.15 |
250.00 |
8. pH |
Glass electrode |
100.00 |
B. Water | . |
|
1. Physical Examination | . | . |
1.1 Total Solids |
Oven-Drying/APHA-AWWA (Sec. 2540) |
200.00 |
2. Chemical Examination | . |
. |
2.1 Acidity |
Titrimetric/APHA-AWWA (Sec. 2310) |
200.00 |
2.2 Alkalinity |
Titrimetric/APHA-AWWA (Sec. 2320) |
200.00 |
2.3 Total Hardness |
EDTA Titrimetric/APHA-AWWA (Sec. 2340) |
200.00 |
2.4 Total Chlorides |
Argentometric APHA-AWWA (Sec. 4500) |
200.00 |
2.5 pH |
Glass electrode |
100.00 |
3. Microbiological Examination | . | . |
3.1 Bacterial Count |
Aerobic plate count | 500.00 |
3.1 Presumptive Test |
Multi-tube Fermentation |
500.00 |
3.1 Confirmatory Test |
Endo-C agar confirmatory test |
500.00 |
| C. Wastewater | ||
1. BOD |
Azide/Manometric (APHA-AWWA-WPCF-EPA) |
500.00 |
2. COD |
Micro COD Dig. & Spec. (APHA-AWWA-EPA) |
500.00 |
3. TSS |
Spectrophotometric APHA-AWWA |
500.00 |
4. Oil & Grease |
Partition-Gravimetric APHA-AWWA (Sec. 5520) |
1,100.00 |
5. pH |
Glass electrode | 100.00 |